Quartz XRD sample holders are used to load quartz samples for X-ray diffraction experiments. During sample preparation, it is essential to ensure that the sample powder is dry, has uniform particle size, and has a flat, tightly packed surface to obtain accurate diffraction data. When using the sample holder, the sample should be placed at the center of the stage, and the sample surface should be tangent to the focusing circle to avoid height errors affecting the test results.
속성 콘텐츠 | 속성 값 |
---|---|
SiO2 | 99.99% |
밀도 | 2.2×10³ kg/cm³ |
경도 | 5.5 - 6.5 모스 스케일 570 KHN 100 |
인장 강도 | 4.8×10⁷ Pa(N/mm2)(7000psi) |
압축 강도 | >1.1×10⁹ Pa(160,000psi) 이상 |
열팽창 계수 | 5.5×10-⁷ cm/cm-°C(20°C-320°C) |
열 전도성 | 1.4W/m-°C |
비열 | 670 J/kg-°C |
연화 포인트 | 1730°C(3146°F) |
어닐링 포인트 | 1210°C(2210°F) |
스트레인 포인트 | 1120°C(2048°F) |
작업 온도 | 1200°C(2192°F) |
전기 저항 | 7×10⁷ 옴 cm(350°C) |
크기 | 사용자 지정 |
로고 | 맞춤형 로고 수락 |
고온 내성
Quartz XRD sample holders are made of quartz glass, which has a softening point of approximately 1730°C. They can be used for extended periods at 1100°C and for short durations at temperatures up to 1450°C.
화학적 안정성
Quartz glass is highly resistant to chemical reactions with most acids. Its acid resistance is approximately 30 times higher than ceramics and 150 times higher than stainless steel. It exhibits exceptional chemical stability, particularly at high temperatures.
낮은 열팽창 계수
Quartz glass has an extremely low coefficient of thermal expansion, allowing it to withstand rapid temperature changes without fracturing. This provides excellent thermal stability.
Good Optical Transmission
Quartz glass exhibits excellent optical transmission across the entire spectrum from ultraviolet to infrared. Its visible light transmission is greater than 93%, and in the ultraviolet spectral region, its transmission can exceed 90%.
애플리케이션 시나리오
Crystal Structure Analysis in Materials Science
Quartz XRD sample holders are crucial in various fields of materials science, especially for crystal structure analysis. By analyzing the diffraction patterns produced from the interaction of X-rays with a material, vital information about the material’s crystal structure, grain size, phase composition, and stress state can be obtained.
Phase Composition and Multi-Phase Material Analysis
Quartz XRD sample holders are used to identify components and their relative proportions within polycrystalline materials such as alloys, ceramics, and composites. They are also important for investigating the local structural characteristics of amorphous materials, such as glass and amorphous alloys.
Phase Transition and Thermal Stability Studies
Quartz XRD sample holders enable the study of phase transition behavior in materials under varying temperature or pressure conditions. By heating or cooling samples and monitoring their diffraction patterns, researchers can determine whether phase transitions occur under specific conditions.
Critical Material Applications in Semiconductor Manufacturing
In the semiconductor industry, quartz XRD sample holders play an important role because of their high-temperature and corrosion-resistant properties. They are used in high-temperature devices, such as furnace tubes and glass boats for diffusion and oxidation processes, and in low-temperature devices, such as quartz rings for etching processes.
When using quartz XRD sample holders for experiments, the following points should be observed:
Ensure the sample holder is clean and free of dust to avoid contaminating the sample and affecting diffraction results.
The sample should be evenly distributed in the sample holder to obtain optimal diffraction signals.
Avoid exposing the sample holder to drastic temperature changes to prevent the quartz glass from cracking due to excessive temperature differentials.
When using the sample holder at high temperatures or under specific conditions, follow the manufacturer’s guidelines and safety regulations.
The following steps can be used to clean and maintain quartz XRD sample holders:
Gently remove dust and residue from the surface of the sample holder using a soft cloth or brush.
For stubborn stains, use a mild detergent and water for cleaning, but ensure thorough rinsing and drying to avoid any chemical residue.
Regularly check the sample holder for cracks or damage, particularly after high-temperature or high-pressure experiments.
Store in a dry, clean place, away from direct sunlight and humid environments.
The lifespan of a quartz XRD sample holder depends on various factors, including:
Usage frequency and experimental conditions; frequent use or use under extreme conditions may shorten its lifespan.
Maintenance and cleanliness of the sample holder; good maintenance can prolong its lifespan.
Material and manufacturing quality of the sample holder; high-quality quartz glass is typically more durable.
자주 묻는 질문
석영 유리는 우수한 물리적 및 화학적 특성, 매우 높은 기계적 경도, 우수한 전기 절연성, 고온 및 내식성, 낮고 안정적인 지연 성능, 우수한 빛 투과율 등을 갖춘 단단하고 부서지기 쉬운 소재입니다. 반도체, 광학, 전기, 화학, 항공우주, 자동차 및 기타 분야에서 널리 사용됩니다. 단단하고 부서지기 쉬운 재료는 가공이 어렵고 많은 분야에서 가장자리 붕괴가 적고 재료 손실이 적으며 단면 거칠기가 낮고 절단 두께 범위가 넓은 절단 공정이 절실히 필요합니다. 석영 유리의 전통적인 절단 방법은 기계식 절단, 즉 휠 절단입니다. 비 전통적인 절단 방법에는 워터젯 절단, 전기 화학 방전 와이어 절단, 연속 레이저 절단 등이 포함됩니다. 기계식 절단은 비용이 저렴하지만 휠과 재료 사이의 접촉으로 인해 공구 마모가 크고 재료가 공구에 의해 쉽게 오염됩니다. 석영 유리는 가장자리 붕괴, 미세 균열 및 잔류 응력이 발생하기 쉬우므로 재료의 강도와 성능에 영향을 미칩니다! 곡선 절단이 어렵고 연마 및 연마와 같은 후처리가 필요합니다. 레이저 절단은 재료에 직접 접촉하지 않고 접촉 응력이 없으며 복잡한 곡선 절단을 수행할 수 있습니다. 피코초 레이저는 작은 스폿 직경, 고정밀, 재료와의 짧은 작용 시간, 작은 작용 면적의 장점을 가지고 있으며 단단하고 부서지기 쉬운 재료의 가공에 적합합니다.
。